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RemDelaporteMathurinRemDelaporteMathurin
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Merge pull request #2 from veliki-filozof/long-samples
Adding long counts
2 parents c6cb67a + bc887f8 commit ba0c3c2

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6 files changed

+318
-46
lines changed

6 files changed

+318
-46
lines changed

‎analysis/tritium/tritium_model.ipynb

Lines changed: 38 additions & 25 deletions
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‎data/general.json

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Original file line numberDiff line numberDiff line change
@@ -167,7 +167,7 @@
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"run_start": "6/18/2025 10:13"
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},
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"tritium_blank_set": {
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"filename": "SLR_BLANK_SCAN.csv",
170+
"filename": "SLR_BLANK_ULTRA_LONG.csv",
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"parameter": "tSIE",
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"blanks": {
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"SLR_BL2" : {
@@ -248,30 +248,30 @@
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"planned_sample_time": "6/18/2025 22:13",
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"actual_sample_time": "6/18/2025 21:33",
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"lsc_vials_filenames": {
251-
"1": "1L_IV_10-1_10-2_OV_10-1_SHORT.csv",
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"2": "1L_IV_10-1_10-2_OV_10-1_SHORT.csv",
253-
"3": "1L_IV_10-1_10-2_OV_10-1_SHORT.csv",
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"4": "1L_IV_10-1_10-2_OV_10-1_SHORT.csv"
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"1": "1L_IV_10-1_10-2_10-3_11-3_11-4_OV_10-1_10-2_11-2.csv",
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"2": "1L_IV_10-1_10-2_10-3_11-3_11-4_OV_10-1_10-2_11-2.csv",
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"3": "1L_IV_10-1_10-2_10-3_11-3_11-4_OV_10-1_10-2_11-2.csv",
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"4": "1L_IV_10-1_10-2_10-3_11-3_11-4_OV_10-1_10-2_11-2.csv"
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}
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},
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"2": {
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"planned_sample_time": "6/19/2025 10:13",
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"actual_sample_time": "6/19/2025 10:26",
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"lsc_vials_filenames": {
261-
"1": "1L_IV_10-1_10-2_OV_10-1_SHORT.csv",
262-
"2": "1L_IV_10-1_10-2_OV_10-1_SHORT.csv",
263-
"3": "1L_IV_10-1_10-2_OV_10-1_SHORT.csv",
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"4": "1L_IV_10-1_10-2_OV_10-1_SHORT.csv"
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"1": "1L_IV_10-1_10-2_10-3_11-3_11-4_OV_10-1_10-2_11-2.csv",
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"2": "1L_IV_10-1_10-2_10-3_11-3_11-4_OV_10-1_10-2_11-2.csv",
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"3": "1L_IV_10-1_10-2_10-3_11-3_11-4_OV_10-1_10-2_11-2.csv",
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"4": "1L_IV_10-1_10-2_10-3_11-3_11-4_OV_10-1_10-2_11-2.csv"
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}
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},
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"3": {
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"planned_sample_time": "6/20/2025 10:13",
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"actual_sample_time": "6/20/2025 08:13",
270270
"lsc_vials_filenames": {
271-
"1": "1L_IV_10-3_OV_10-2_SHORT.csv",
272-
"2": "1L_IV_10-3_OV_10-2_SHORT.csv",
273-
"3": "1L_IV_10-3_OV_10-2_SHORT.csv",
274-
"4": "1L_IV_10-3_OV_10-2_SHORT.csv"
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"1": "1L_IV_10-1_10-2_10-3_11-3_11-4_OV_10-1_10-2_11-2.csv",
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"2": "1L_IV_10-1_10-2_10-3_11-3_11-4_OV_10-1_10-2_11-2.csv",
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"3": "1L_IV_10-1_10-2_10-3_11-3_11-4_OV_10-1_10-2_11-2.csv",
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"4": "1L_IV_10-1_10-2_10-3_11-3_11-4_OV_10-1_10-2_11-2.csv"
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}
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}
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},
@@ -280,20 +280,20 @@
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"planned_sample_time": "6/19/2025 10:13",
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"actual_sample_time": "6/19/2025 10:26",
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"lsc_vials_filenames": {
283-
"1": "1L_IV_10-1_10-2_OV_10-1_SHORT.csv",
284-
"2": "1L_IV_10-1_10-2_OV_10-1_SHORT.csv",
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"3": "1L_IV_10-1_10-2_OV_10-1_SHORT.csv",
286-
"4": "1L_IV_10-1_10-2_OV_10-1_SHORT.csv"
283+
"1": "1L_IV_10-1_10-2_10-3_11-3_11-4_OV_10-1_10-2_11-2.csv",
284+
"2": "1L_IV_10-1_10-2_10-3_11-3_11-4_OV_10-1_10-2_11-2.csv",
285+
"3": "1L_OV_11-8-3_-3-3_OV_10-2-3_-1-3_ULTRA_LONG.csv",
286+
"4": "1L_IV_10-1_10-2_10-3_11-3_11-4_OV_10-1_10-2_11-2.csv"
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}
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},
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"2": {
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"planned_sample_time": "6/20/2025 10:13",
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"actual_sample_time": "6/20/2025 08:13",
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"lsc_vials_filenames": {
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"1": "1L_IV_10-3_OV_10-2_SHORT.csv",
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"2": "1L_IV_10-3_OV_10-2_SHORT.csv",
295-
"3": "1L_IV_10-3_OV_10-2_SHORT.csv",
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"4": "1L_IV_10-3_OV_10-2_SHORT.csv"
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"1": "1L_IV_10-1_10-2_10-3_11-3_11-4_OV_10-1_10-2_11-2.csv",
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"2": "1L_IV_10-1_10-2_10-3_11-3_11-4_OV_10-1_10-2_11-2.csv",
295+
"3": "1L_OV_11-8-3_-3-3_OV_10-2-3_-1-3_ULTRA_LONG.csv",
296+
"4": "1L_IV_10-1_10-2_10-3_11-3_11-4_OV_10-1_10-2_11-2.csv"
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}
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}
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}

‎data/tritium_detection/1L_11_ULTRA_LONG_TEST.csv

Lines changed: 59 additions & 0 deletions
Original file line numberDiff line numberDiff line change
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Assay Definition
2+
3+
Assay Description:
4+
1L BABY Experiment standard count, beginning with run 1L-3
5+
Assay Type: DPM (Single)
6+
Report Name: Standard report
7+
Output Data Path: C:\Packard\TriCarb\Results\Default\NEW_Flibe_Long\Various
8+
Raw Results Path: C:\Packard\Tricarb\Results\Default\NEW_Flibe_Long\20250714_2344\20250714_2344.results
9+
Comma-Delimited File Name: C:\Packard\TriCarb\Results\Default\NEW_Flibe_Long\Various\1L_11_ULTRA_LONG_TEST.csv
10+
Assay File Name: C:\Packard\TriCarb\Assays\NEW_Flibe_Long.lsa
11+
12+
Additional Data Files Generated with this Protocol:
13+
Standard report
14+
[Excel] 1L_11_ULTRA_LONG_TEST.csv
15+
16+
17+
Count Conditions
18+
19+
Nuclide: LIBRA UG LLT NM
20+
Quench Indicator: tSIE
21+
External Std Terminator (sec): 0.5 2s%
22+
Pre-Count Delay (min): 0.00
23+
Quench Set:
24+
Low Energy: 3H-UG-LLT-NM-C
25+
Count Time (min): 500.00
26+
Count Mode: Normal
27+
Assay Count Cycles: 1 Repeat Sample Count: 1
28+
Number of Vials/Sample: 1 Calculate % Reference: Off
29+
30+
31+
Background Subtract: Off
32+
Low CPM Threshold: Off
33+
2 Sigma % Terminator: Off
34+
35+
Regions LL UL
36+
A 0.5 5.0
37+
B 0.5 10.0
38+
C 0.0 18.6
39+
40+
41+
Count Corrections
42+
43+
Static Controller: On Luminescence Correction: On GCT: n/a
44+
Colored Samples: Off Heterogeneity Monitor: Off PAC: Disabled
45+
Coincidence Time (nsec): 18 Delay Before Burst (nsec): 75 PAC Strength: n/a Auxiliary Spectrum: n/a
46+
47+
48+
S#,SMPL_ID,Bq:1,CPMA,A:2S%,LUM,tSIE,Eff Nuc1 In A,Count Time,DPM1
49+
1,BLANK,0.271,4.060,4.50,0,290.50,25.01,500,16.236
50+
Missing vial 2.
51+
3,1L-OV_11-7-3,0.459,7.062,3.40,0,298.22,25.67,500,27.513
52+
Missing vial 4.
53+
5,1L-OV_11-7-1,0.206,3.700,4.73,0,366.33,29.99,500,12.336
54+
Missing vial 6.
55+
7,1L-IV_11-8-3,0.469,7.082,3.39,0,292.09,25.14,500,28.168
56+
Missing vial 8.
57+
9,1L-IV_11-8-1,0.222,3.800,4.66,0,340.67,28.59,500,13.290
58+
Missing vial 10.
59+
11,SLR_BL11,0.310,4.352,4.34,0,272.30,23.41,500,18.594

‎data/tritium_detection/1L_IV_10-1_10-2_10-3_11-3_11-4_OV_10-1_10-2_11-2.csv

Lines changed: 87 additions & 0 deletions
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Assay Definition
2+
3+
Assay Description:
4+
1L BABY Experiment standard count, beginning with run 1L-3
5+
Assay Type: DPM (Single)
6+
Report Name: Standard report
7+
Output Data Path: C:\Packard\Tricarb\Results\Default\NEW_Flibe_Long\20250624_0919\Replay_20250626_181729
8+
Raw Results Path: C:\Packard\Tricarb\Results\Default\NEW_Flibe_Long\20250624_0919\20250624_0919.results
9+
Comma-Delimited File Name: C:\Packard\Tricarb\Results\Default\NEW_Flibe_Long\20250624_0919\Replay_20250626_181729\1L_IV_10-1_10-2_10-3_11-3_11-4_OV_10-1_10-2_11-2.csv
10+
Assay File Name: C:\Packard\TriCarb\Assays\NEW_Flibe_Long.lsa
11+
12+
Additional Data Files Generated with this Protocol:
13+
Standard report
14+
[Excel] 1L_IV_10-1_10-2_10-3_11-3_11-4_OV_10-1_10-2_11-2.csv
15+
16+
17+
Count Conditions
18+
19+
Nuclide: LIBRA UG LLT NM
20+
Quench Indicator: tSIE
21+
External Std Terminator (sec): 0.5 2s%
22+
Pre-Count Delay (min): 0.00
23+
Quench Set:
24+
Low Energy: 3H-UG-LLT-NM-C
25+
Count Time (min): 100.00
26+
Count Mode: Normal
27+
Assay Count Cycles: 1 Repeat Sample Count: 1
28+
Number of Vials/Sample: 1 Calculate % Reference: Off
29+
30+
31+
Background Subtract: Off
32+
Low CPM Threshold: Off
33+
2 Sigma % Terminator: Off
34+
35+
Regions LL UL
36+
A 0.5 5.0
37+
B 0.5 10.0
38+
C 0.0 18.6
39+
40+
41+
Count Corrections
42+
43+
Static Controller: On Luminescence Correction: On GCT: n/a
44+
Colored Samples: Off Heterogeneity Monitor: Off PAC: Disabled
45+
Coincidence Time (nsec): 18 Delay Before Burst (nsec): 75 PAC Strength: n/a Auxiliary Spectrum: n/a
46+
47+
48+
S#,SMPL_ID,Bq:1,CPMA,A:2S%,LUM,tSIE,Eff Nuc1 In A,Count Time,DPM1
49+
1,1L-IV_10-1-1,0.283,4.400,9.64,0,300.92,25.90,100,16.989
50+
2,1L-IV_10-1-2,0.278,4.220,9.85,0,293.80,25.29,100,16.687
51+
3,1L-IV_10-1-3,4.739,72.330,2.35,0,295.55,25.44,100,284.323
52+
4,1L-IV_10-1-4,0.374,5.590,8.55,0,289.77,24.94,100,22.411
53+
Missing vial 5.
54+
6,1L-IV_10-2-1,0.243,3.830,10.38,0,305.24,26.27,100,14.579
55+
7,1L-IV_10-2-2,0.272,4.110,9.98,0,292.66,25.19,100,16.315
56+
8,1L-IV_10-2-3,0.634,9.690,6.45,0,295.74,25.46,100,38.066
57+
9,1L-IV_10-2-4,0.306,4.630,9.39,0,292.97,25.22,100,18.360
58+
Missing vial 10.
59+
11,1L-IV_10-3-1,0.240,3.830,10.33,0,309.25,26.61,100,14.391
60+
12,1L-IV_10-3-2,0.278,4.250,9.79,0,295.84,25.46,100,16.691
61+
13,1L-IV_10-3-3,0.350,5.230,8.83,0,289.35,24.91,100,20.998
62+
14,1L-IV_10-3-4,0.259,3.940,10.20,0,294.89,25.38,100,15.523
63+
Missing vial 15.
64+
16,1L-OV_10-1-1,0.261,4.300,9.73,0,321.68,27.47,100,15.652
65+
17,1L-OV_10-1-2,0.286,4.340,9.64,0,293.68,25.28,100,17.168
66+
18,1L-OV_10-1-3,0.849,12.810,5.61,0,292.29,25.16,100,50.916
67+
19,1L-OV_10-1-4,0.321,4.860,9.17,0,293.02,25.22,100,19.269
68+
Missing vial 20.
69+
21,1L-OV_10-2-1,0.245,3.990,10.09,0,315.28,27.09,100,14.726
70+
22,1L-OV_10-2-2,0.278,4.170,9.93,0,290.77,25.03,100,16.661
71+
23,1L-OV_10-2-3,0.628,9.500,6.52,0,293.04,25.22,100,37.663
72+
24,1L-OV_10-2-4,0.309,4.700,9.32,0,294.24,25.33,100,18.558
73+
Missing vial 25.
74+
26,1L-IV_11-3-1,0.251,4.040,10.05,0,311.54,26.81,100,15.068
75+
27,1L-IV_11-3-2,0.301,4.570,9.46,0,294.30,25.33,100,18.041
76+
28,1L-IV_11-3-3,0.343,5.180,8.87,0,292.65,25.19,100,20.563
77+
29,1L-IV_11-3-4,0.302,4.550,9.46,0,291.75,25.11,100,18.118
78+
Missing vial 30.
79+
31,1L-OV_11-2-1,0.251,4.130,9.94,0,320.00,27.37,100,15.088
80+
32,1L-OV_11-2-2,0.279,4.260,9.78,0,295.93,25.47,100,16.725
81+
33,1L-OV_11-2-3,0.535,8.130,7.05,0,294.11,25.32,100,32.115
82+
34,1L-OV_11-2-4,0.290,4.410,9.63,0,294.69,25.37,100,17.386
83+
Missing vial 35.
84+
36,1L-IV_11-4-1,0.235,3.990,10.21,0,335.38,28.28,100,14.109
85+
37,1L-IV_11-4-2,0.258,3.940,10.23,0,295.23,25.41,100,15.505
86+
38,1L-IV_11-4-3,0.390,5.890,8.32,0,292.29,25.16,100,23.411
87+
39,1L-IV_11-4-4,0.301,4.570,9.48,0,294.17,25.32,100,18.049

‎data/tritium_detection/1L_OV_11-8-3_-3-3_OV_10-2-3_-1-3_ULTRA_LONG.csv

Lines changed: 55 additions & 0 deletions
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Assay Definition
2+
3+
Assay Description:
4+
1L BABY Experiment standard count, beginning with run 1L-3
5+
Assay Type: DPM (Single)
6+
Report Name: Standard report
7+
Output Data Path: C:\Packard\Tricarb\Results\Default\NEW_Flibe_Long\20250719_2018\Replay_20250721_133815
8+
Raw Results Path: C:\Packard\Tricarb\Results\Default\NEW_Flibe_Long\20250719_2018\20250719_2018.results
9+
Comma-Delimited File Name: C:\Packard\Tricarb\Results\Default\NEW_Flibe_Long\20250719_2018\Replay_20250721_133815\1L_OV-11-8-3_-3-3_OV-10-2-3_-1-3_ULTRA_LONG.csv
10+
Assay File Name: C:\Packard\TriCarb\Assays\NEW_Flibe_Long.lsa
11+
12+
Additional Data Files Generated with this Protocol:
13+
Standard report
14+
[Excel] 1L_OV-11-8-3_-3-3_OV-10-2-3_-1-3_ULTRA_LONG.csv
15+
16+
17+
Count Conditions
18+
19+
Nuclide: LIBRA UG LLT NM
20+
Quench Indicator: tSIE
21+
External Std Terminator (sec): 0.5 2s%
22+
Pre-Count Delay (min): 0.00
23+
Quench Set:
24+
Low Energy: 3H-UG-LLT-NM-C
25+
Count Time (min): 500.00
26+
Count Mode: Normal
27+
Assay Count Cycles: 1 Repeat Sample Count: 1
28+
Number of Vials/Sample: 1 Calculate % Reference: Off
29+
30+
31+
Background Subtract: Off
32+
Low CPM Threshold: Off
33+
2 Sigma % Terminator: Off
34+
35+
Regions LL UL
36+
A 0.5 5.0
37+
B 0.5 10.0
38+
C 0.0 18.6
39+
40+
41+
Count Corrections
42+
43+
Static Controller: On Luminescence Correction: On GCT: n/a
44+
Colored Samples: Off Heterogeneity Monitor: Off PAC: Disabled
45+
Coincidence Time (nsec): 18 Delay Before Burst (nsec): 75 PAC Strength: n/a Auxiliary Spectrum: n/a
46+
47+
48+
S#,SMPL_ID,Bq:1,CPMA,A:2S%,LUM,tSIE,Eff Nuc1 In A,Count Time,DPM1
49+
1,1L-OV_11-3-3,0.635,9.652,2.90,0,294.35,25.34,500,38.096
50+
Missing vial 2.
51+
3,1L-OV_10-2-3,0.610,9.270,2.96,0,294.16,25.32,500,36.612
52+
Missing vial 4.
53+
5,1L-OV_10-1-3,0.788,11.924,2.60,0,293.17,25.23,500,47.252
54+
Missing vial 6.
55+
7,1L-OV_11-8-3,0.399,5.956,3.73,0,289.06,24.88,500,23.937

‎data/tritium_detection/SLR_BLANK_ULTRA_LONG.csv

Lines changed: 58 additions & 0 deletions
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Assay Definition
2+
3+
Assay Description:
4+
1L BABY Experiment standard count, beginning with run 1L-3
5+
Assay Type: DPM (Single)
6+
Report Name: Standard report
7+
Output Data Path: C:\Packard\Tricarb\Results\Default\NEW_Flibe_Long\20250711_1132\Replay_20250717_175208
8+
Raw Results Path: C:\Packard\Tricarb\Results\Default\NEW_Flibe_Long\20250711_1132\20250711_1132.results
9+
Comma-Delimited File Name: C:\Packard\Tricarb\Results\Default\NEW_Flibe_Long\20250711_1132\Replay_20250717_175208\SLR_BLANK_ULTRA_LONG.csv
10+
Assay File Name: C:\Packard\TriCarb\Assays\NEW_Flibe_Long.lsa
11+
12+
Additional Data Files Generated with this Protocol:
13+
Standard report
14+
[Excel] SLR_BLANK_ULTRA_LONG.csv
15+
16+
17+
Count Conditions
18+
19+
Nuclide: LIBRA UG LLT NM
20+
Quench Indicator: tSIE
21+
External Std Terminator (sec): 0.5 2s%
22+
Pre-Count Delay (min): 0.00
23+
Quench Set:
24+
Low Energy: 3H-UG-LLT-NM-C
25+
Count Time (min): 500.00
26+
Count Mode: Normal
27+
Assay Count Cycles: 1 Repeat Sample Count: 1
28+
Number of Vials/Sample: 1 Calculate % Reference: Off
29+
30+
31+
Background Subtract: Off
32+
Low CPM Threshold: Off
33+
2 Sigma % Terminator: Off
34+
35+
Regions LL UL
36+
A 0.5 5.0
37+
B 0.5 10.0
38+
C 0.0 18.6
39+
40+
41+
Count Corrections
42+
43+
Static Controller: On Luminescence Correction: On GCT: n/a
44+
Colored Samples: Off Heterogeneity Monitor: Off PAC: Disabled
45+
Coincidence Time (nsec): 18 Delay Before Burst (nsec): 75 PAC Strength: n/a Auxiliary Spectrum: n/a
46+
47+
48+
S#,SMPL_ID,Bq:1,CPMA,A:2S%,LUM,tSIE,Eff Nuc1 In A,Count Time,DPM1
49+
1,FAIL,0.302,4.270,9.81,0,273.68,23.53,100,18.149
50+
2,SLR_BL10,0.279,4.136,4.47,0,287.51,24.75,500,16.713
51+
3,SLR_BL9,0.254,3.970,4.55,0,302.12,26.00,500,15.267
52+
4,SLR_BL8,0.232,3.810,4.64,0,320.58,27.41,500,13.902
53+
5,SLR_BL6,0.216,3.838,4.63,0,360.24,29.66,500,12.939
54+
6,SLR_BL4,0.177,3.430,4.90,0,414.19,32.33,500,10.610
55+
7,SLR_BL2,0.163,3.342,4.96,0,480.58,34.10,500,9.801
56+
Missing vial 8.
57+
9,SLR_BL11,0.310,4.352,4.34,0,272.30,23.41,500,18.594
58+
NOTE: Vial 9 manually copied from 1L_11_ULTRA_LONG_TEST

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